Monthly Archives: August 2021

  1. ICP Standards: Guide to Washout Considerations

    Inductively coupled plasma (ICP) mass spectrometry is a form of mass spectrometry that employs inductively coupled plasma to ionize a sample. It atomizes the sample and forms atomic and small polyatomic ions which can then be detected.

    ICP standards are used in ICP-OES, which is a trace-level, elemental analysis method that uses the emission spectra of a sample to recognize and quantify the elements present. The involved elements can be recognized by their characteristic emission lines and quantified by the intensity of the same lines. Trace analysis is often thought of as an analyte concentration low enough to cause challenges. The challenges may be caused by the sample size, matrix, or washout issues.

    What Can be Done about Washout?

    Washout refers to sample solution being removed from the sample introduction system during analysis. Ensuring that the previous sample has been completely removed before introducing the next sample for analysis will eliminate

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  2. Custom CRMs for Water Testing: Bringing Precision to the Pt-Co Method

    Water testing regulations—though stringent—have historically lacked an element of precision. In the past, it was sufficient to evaluate the color of water and wastewater according to a grading known as water-white. This was a general evaluation for solvents that have the appearance of clear water. It was an inaccurate technique that was made worse as different expressions of the terminology arose over time, meaning there was no universal standard for what water-white actually entailed.

    Custom CRMs (Certified Reference Materials) have helped innovate water and wastewater testing by introducing unprecedented levels of precision to the workflow. But before we explore the role of custom CRMs in water testing, it is worthwhile looking at the innovative method that replaced the water-white colorimetric scale. 

    What is the Platinum-Cobalt Method?

    A new colorimetric scale was introduced to resolve the issues associated with water-white. Drawing from an index orig

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