Sample Preparation - Potassium pyrosulfate fusion of titanium oxide

 
What are the proper temperature and time in the fusion process?
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For this application, the flux to sample ratio should be approximately 20:1, the temperature 500 C, and the time about 20 minutes. If the flux begins to solidify, add concentrated H2SO4 dropwise to regenerate.

Posted: 06/14/19 09:45:46

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