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Method Validation

Trace Analysis Guide:
Part 17

By Paul Gaines, Ph.D.
OverviewPurpose of Method ValidationReferences: The Validation ProcessConfirm Basic Performance CriteriaRobustnessCollaborative and Cooperative TestingConcluding StatementFurther Reading
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References: The Validation Process

There are numerous publications addressing this issue. Following are some references you may find useful:

Trace Analysis: A structured approach to obtaining reliable results; Prichard, E., Mackay, G. M., Points, J., Eds.; The Royal Society of Chemistry: 31-39; 1996.

A Practical Guide to Method Validation; Green, J. Mark, Ed.; Analytical Chemistry (68): 305A-309A; 1996.

Swartz, Michael E.; Krull, Ira S. Analytical Method Development and Validation; Marcel Dekker, Inc.: 1997.

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Trace Analysis Guide
Table of Contents 1. Definition, Stages and Training 2. Planning the Project 3. Sampling and Subsampling 4. Introduction to Sample Preparation 5. Container Material Properties 6. Container Transpiration 7. Stability of Elements at ppb Concentration Levels 8. Environmental Contamination 9. Contamination From Reagents 10. Contamination From the Analyst and Apparatus 11. Acid Digestions of Inorganic Samples 12. Acid Digestions of Organic Samples 13. Sample Preparation by Fusion 14. Ashing Sample Preparation Procedures 15. ICP-OES Measurement 16. ICP-MS Measurement 17. Method Validation
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