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Method Validation

Trace Analysis Guide:
Part 17

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Collaborative and Cooperative Testing

This is an activity or component of method validation that is performed by organizations that develop standard methods of chemical analysis such as ASTM and AOAC. It is also an activity that is performed by large corporations with multiple testing locations. The term reproducibility is used to describe interlaboratory precision and is expressed as standard deviation. Different organizations use different processes, some more convenient than others. For this reason, refer to the following references:

Validation of Analytical Methods; Taylor, J.K., Ed.; Analytical Chemistry (55): 600A-608A; 1983.

The Role of Collaborative and Cooperative Studies in Evaluation of Analytical Methods; Taylor, J.K., Ed.; J. Assoc. Off. Anal. Chem. (69): p. 398; 1986.

Youden, W.J.; Steiner, E. H. Steiner Statistical Manual of the AOAC; AOAC: Arlington, VA, 1975; 5th printing 1987.

ASTM Method E691-92; Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method; ASTM: Philadelphia, PA.

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